# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2008src0886 _shelx_title ' 2008src0886 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 339.12 _exptl_crystal_F_000 1362.00 _reflns_d_resolution_high 0.7700 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.1766 _cell_length_b 14.4577 _cell_length_c 15.1547 _cell_angle_alpha 76.818 _cell_angle_beta 79.622 _cell_angle_gamma 73.510 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12080.22 11803.79 223.30 o 3 0 0 2221.51 2126.48 40.52 o 4 0 0 3172.98 3118.77 44.56 o 5 0 0 7201.65 6976.07 89.29 o 6 0 0 295.83 280.21 17.32 o 7 0 0 2701.84 2866.12 48.23 o 8 0 0 2017.62 1908.30 43.50 o 9 0 0 3950.84 3916.04 87.76 o 10 0 0 2115.18 2106.74 68.03 o 11 0 0 780.50 923.19 58.99 o 12 0 0 3424.46 3306.00 130.48 o 13 0 0 130.49 255.11 73.72 o 14 0 0 10873.31 10544.14 466.62 o 15 0 0 1437.14 1121.82 190.09 o -14 1 0 685.85 752.44 106.69 o -13 1 0 8054.09 7976.33 499.45 o -12 1 0 887.27 796.59 137.46 o -11 1 0 165.95 153.87 34.80 o -10 1 0 466.49 462.72 80.70 o -9 1 0 415.08 327.10 38.54 o -8 1 0 8500.66 8835.74 151.38 o -7 1 0 6117.18 6173.07 122.68 o -6 1 0 25586.71 26191.85 313.99 o -5 1 0 25983.88 24899.46 311.07 o -4 1 0 56652.13 55399.04 648.02 o -3 1 0 44577.31 43460.53 579.88 o -2 1 0 203.51 147.56 18.85 o 3 1 0 10454.19 10212.86 129.96 o 4 1 0 6373.72 6458.32 89.86 o 5 1 0 7325.03 7376.25 98.11 o 6 1 0 2433.22 2427.58 42.45 o 7 1 0 5268.40 5569.37 80.25 o 8 1 0 2366.60 2258.01 51.36 o 9 1 0 21823.38 21543.96 295.93 o 10 1 0 4373.70 4504.79 86.25 o 11 1 0 35953.98 37208.67 765.95 o 12 1 0 245.44 240.34 44.78 o 13 1 0 9385.98 9411.73 383.55 o 14 1 0 660.41 606.95 69.17 o 15 1 0 2360.06 1959.40 205.24 o -14 2 0 15.05 120.45 109.61 o -13 2 0 51.53 187.92 83.60 o -12 2 0 3.52 29.21 60.40 o -11 2 0 2802.97 2937.26 120.77 o -10 2 0 10.89 -18.57 36.84 o -9 2 0 17428.53 17203.57 307.89 o -8 2 0 7819.76 7664.87 139.86 o -7 2 0 15053.14 15057.62 215.43 o -6 2 0 44757.49 44060.05 730.14 o -5 2 0 495.37 620.82 30.01 o -4 2 0 103886.66 100623.85 1588.74 o -3 2 0 4127.97 4320.61 74.29 o -2 2 0 15511.88 14846.60 221.21 o -1 2 0 1367.93 1623.48 80.28 o 1 2 0 56.05 96.30 12.19 o 2 2 0 17.28 -18.89 12.60 o 3 2 0 13321.55 13315.17 178.31 o 4 2 0 17651.83 17975.81 230.00 o 5 2 0 42988.26 42791.24 580.52 o 6 2 0 1617.16 1819.93 62.12 o 7 2 0 7128.53 6773.86 117.41 o 8 2 0 22380.32 23228.88 308.71 o 9 2 0 374.65 411.97 23.12 o 10 2 0 23967.35 24395.86 455.99 o 11 2 0 10648.69 10592.48 251.29 o 12 2 0 14212.05 14070.95 380.83 o 13 2 0 5706.50 5672.62 212.31 o 14 2 0 1282.41 1251.56 103.05 o 15 2 0 1688.35 1726.56 139.61 o -14 3 0 329.54 347.19 83.47 o -13 3 0 2.88 32.43 85.09 o -12 3 0 8005.96 8197.04 246.79 o -11 3 0 842.26 901.49 76.98 o -10 3 0 21994.79 22127.94 487.66 o -9 3 0 25725.66 25822.79 429.66 o -8 3 0 14148.06 13974.57 226.16 o -7 3 0 17262.73 17426.89 247.33 o -6 3 0 35.89 116.67 29.48 o -5 3 0 29574.48 28828.40 391.92 o -4 3 0 12252.26 12269.63 179.63 o -3 3 0 158.44 229.77 19.10 o -2 3 0 3443.80 3408.52 74.48 o -1 3 0 17073.10 17019.49 269.45 o 0 3 0 5106.80 5212.39 84.24 o 1 3 0 55.48 75.21 9.47 o 2 3 0 12990.17 12713.14 194.03 o 3 3 0 21368.27 20866.28 308.77 o 4 3 0 21518.47 21685.37 270.45 o 5 3 0 27762.82 26994.82 313.17 o 6 3 0 13671.35 13559.16 157.12 o 7 3 0 53266.05 54355.07 632.06 o 8 3 0 14.80 35.41 12.75 o 9 3 0 21493.63 22102.28 326.46 o 10 3 0 97.92 127.04 33.77 o 11 3 0 5100.50 5077.26 100.95 o 12 3 0 1805.23 1770.92 85.13 o 13 3 0 4.92 9.52 51.09 o 14 3 0 38.26 128.99 66.10 o 15 3 0 27.33 -43.58 70.79 o -13 4 0 4839.49 4947.24 262.06 o -12 4 0 2562.59 2433.91 150.92 o -11 4 0 4652.42 4609.20 200.44 o -10 4 0 19382.37 19062.15 514.89 o -9 4 0 1292.37 1205.51 134.28 o -8 4 0 27407.27 27752.34 574.66 o -7 4 0 31.04 53.88 27.99 o -6 4 0 13539.39 13991.81 256.04 o -5 4 0 4529.46 4595.44 105.35 o -4 4 0 32.28 30.75 19.63 o -3 4 0 1053.76 1021.88 34.50 o -2 4 0 1578.56 1729.08 47.63 o -1 4 0 4202.18 4116.06 64.57 o 0 4 0 416.50 493.12 16.49 o 1 4 0 75172.39 69991.09 886.13 o 2 4 0 18239.36 17663.87 280.38 o 3 4 0 16359.52 16046.39 280.20 o 4 4 0 78833.57 75971.78 1061.56 o 5 4 0 10862.88 10961.20 152.42 o 6 4 0 9030.37 8427.00 134.01 o 7 4 0 9475.10 9849.66 121.49 o 8 4 0 4247.78 4420.44 73.48 o 9 4 0 444.02 443.98 30.57 o 10 4 0 1775.60 1938.03 49.60 o 11 4 0 520.06 547.84 34.71 o 12 4 0 493.06 466.58 53.53 o 13 4 0 2641.37 2823.77 190.65 o 14 4 0 1125.07 1094.20 138.14 o 15 4 0 1781.93 1640.31 209.49 o -13 5 0 5023.40 4126.10 311.56 o -12 5 0 4680.76 4774.62 174.33 o -11 5 0 9527.44 9503.21 371.61 o -10 5 0 2382.89 2125.62 120.99 o -9 5 0 10921.76 11141.98 501.99 o -8 5 0 9.91 66.00 44.03 o -7 5 0 4.95 50.32 33.41 o -6 5 0 342.28 400.95 35.56 o -5 5 0 2051.14 2307.96 57.56 o -4 5 0 9454.10 9655.93 143.93 o -3 5 0 205.78 220.08 22.95 o -2 5 0 7585.15 7511.84 135.26 o -1 5 0 10446.32 10243.63 141.50 o 0 5 0 28411.15 27208.09 363.90 o 1 5 0 36345.85 35970.57 408.11 o 2 5 0 6199.68 6118.77 94.01 o 3 5 0 66161.24 63827.71 931.17 o 4 5 0 3.33 46.29 13.28 o 5 5 0 33906.58 33905.31 430.68 o 6 5 0 105.80 203.89 20.94 o 7 5 0 830.68 799.24 30.98 o 8 5 0 154.60 227.99 19.66 o 9 5 0 7160.06 7301.68 126.41 o 10 5 0 6767.34 6735.62 139.80 o 11 5 0 266.80 291.90 23.05 o 12 5 0 11274.53 11169.77 345.75 o 13 5 0 3620.28 3587.98 188.54 o 14 5 0 7818.21 7862.01 445.54 o 15 5 0 6575.20 6258.50 311.96 o -12 6 0 3137.82 2742.07 168.55 o -11 6 0 66.89 60.28 52.77 o -10 6 0 717.56 703.00 133.50 o -9 6 0 426.44 622.35 89.15 o -8 6 0 35.16 20.13 46.47 o -7 6 0 8022.57 7974.07 213.01 o -6 6 0 1655.82 1797.79 67.77 o -5 6 0 35691.93 36020.23 593.42 o -4 6 0 4492.88 4714.13 94.98 o -3 6 0 44021.83 43841.70 613.91 o -2 6 0 27153.16 27338.39 444.10 o -1 6 0 13112.80 13200.24 181.36 o 0 6 0 20519.99 19948.14 242.04 o 1 6 0 4661.37 4455.97 64.68 o 2 6 0 14400.27 14042.06 186.25 o 3 6 0 6075.95 6122.58 107.89 o 4 6 0 2793.25 2670.80 55.66 o 5 6 0 5.53 28.29 14.91 o 6 6 0 569.86 616.60 21.42 o 7 6 0 195.04 256.42 23.64 o 8 6 0 1329.85 1445.50 48.21 o 9 6 0 15938.83 16460.46 244.68 o 10 6 0 111.04 140.73 21.93 o 11 6 0 13625.63 13713.30 343.05 o 12 6 0 8569.44 9230.16 311.00 o 13 6 0 6934.22 7165.80 330.28 o 14 6 0 19412.68 19618.62 1409.16 o 15 6 0 382.23 401.26 84.33 o -12 7 0 313.53 330.89 92.96 o -11 7 0 295.35 192.39 81.63 o -10 7 0 61.64 122.24 58.55 o -9 7 0 4558.69 4602.76 230.53 o -8 7 0 14626.64 13980.73 715.06 o -7 7 0 537.16 586.17 69.03 o -6 7 0 29434.98 28628.96 665.71 o -5 7 0 9375.50 9768.86 188.26 o -4 7 0 34112.94 34629.23 446.67 o -3 7 0 17598.55 17911.96 321.29 o -2 7 0 1495.84 1653.32 53.74 o -1 7 0 31262.49 31568.28 440.41 o 0 7 0 3262.66 3563.59 81.22 o 1 7 0 1808.23 1836.56 37.84 o 2 7 0 2669.65 2891.25 47.99 o 3 7 0 988.00 1024.92 34.11 o 4 7 0 4985.69 4906.68 89.08 o 5 7 0 103.45 89.83 23.78 o 6 7 0 13322.35 13375.57 206.84 o 7 7 0 47.27 72.31 18.22 o 8 7 0 39234.80 40121.48 598.66 o 9 7 0 4967.68 4941.94 113.89 o 10 7 0 12346.46 12852.32 261.40 o 11 7 0 5641.90 5462.77 176.84 o 12 7 0 3142.57 2856.37 142.68 o 13 7 0 7721.46 8610.79 367.42 o 14 7 0 347.33 274.47 85.34 o 15 7 0 1893.59 1724.04 214.88 o -11 8 0 6196.77 6021.19 274.54 o -10 8 0 1805.67 1706.56 102.66 o -9 8 0 9563.06 9512.64 293.42 o -8 8 0 509.05 596.31 56.43 o -7 8 0 18600.50 19227.69 483.87 o -6 8 0 4152.24 4083.14 129.04 o -5 8 0 36712.93 37207.48 709.01 o -4 8 0 12877.90 13384.91 228.16 o -3 8 0 2072.82 2272.45 66.68 o -2 8 0 4233.86 4412.86 117.49 o -1 8 0 2094.99 2165.59 52.22 o 0 8 0 2185.58 2414.43 52.42 o 1 8 0 1458.97 1606.34 46.84 o 2 8 0 9140.90 9360.64 119.22 o 3 8 0 23471.66 23695.11 356.56 o 4 8 0 3092.24 3266.69 63.24 o 5 8 0 43593.87 44040.74 618.54 o 6 8 0 4910.81 5098.15 99.78 o 7 8 0 11399.83 11300.99 189.68 o 8 8 0 20277.14 20357.51 347.75 o 9 8 0 6668.45 6821.83 150.69 o 10 8 0 10955.27 11410.13 288.73 o 11 8 0 3238.91 3214.23 125.13 o 12 8 0 7276.47 7150.09 306.96 o 13 8 0 163.34 31.51 93.29 o 14 8 0 11.34 238.62 130.90 o 15 8 0 2.79 61.17 68.48 o -11 9 0 167.13 144.65 66.36 o -10 9 0 9366.40 8939.44 418.20 o -9 9 0 92.97 55.16 101.66 o -8 9 0 6359.02 6188.87 295.69 o -7 9 0 9692.74 9751.27 318.39 o -6 9 0 74.16 135.15 37.58 o -5 9 0 8374.69 8465.75 206.14 o -4 9 0 6355.65 6506.17 147.67 o -3 9 0 3212.42 3250.56 80.95 o -2 9 0 1216.50 1301.51 60.54 o -1 9 0 5113.04 5393.11 106.28 o 0 9 0 3835.59 3902.73 80.28 o 1 9 0 5360.06 5396.59 87.83 o 2 9 0 23020.60 23779.36 320.48 o 3 9 0 447.76 498.49 29.26 o 4 9 0 63006.88 62543.98 1044.98 o 5 9 0 2866.90 2793.95 75.66 o 6 9 0 20706.46 21002.19 352.72 o 7 9 0 14385.08 14460.19 237.49 o 8 9 0 3614.27 3598.09 84.75 o 9 9 0 12706.59 12575.63 411.79 o 10 9 0 710.42 728.13 55.38 o 11 9 0 1120.78 974.13 79.01 o 12 9 0 1012.32 1231.40 110.45 o 13 9 0 1126.63 1053.51 177.37 o 14 9 0 394.62 376.97 77.10 o 15 9 0 693.55 672.00 93.48 o -10 10 0 2920.42 2913.94 148.04 o -9 10 0 4789.35 4506.20 306.20 o -8 10 0 1387.83 1193.09 161.97 o -7 10 0 559.18 643.32 96.52 o -6 10 0 242.21 324.06 61.22 o -5 10 0 98.56 138.16 38.00 o -4 10 0 99.93 147.72 34.63 o -3 10 0 5152.11 5169.01 156.73 o -2 10 0 27416.52 28587.60 542.77 o -1 10 0 49691.34 50446.83 995.62 o 0 10 0 1884.70 1949.57 61.12 o 1 10 0 25318.96 25928.30 528.95 o 2 10 0 155.04 222.61 30.13 o 3 10 0 23392.85 23122.12 319.96 o 4 10 0 21856.01 21662.06 340.12 o 5 10 0 7630.03 7668.77 135.73 o 6 10 0 8127.35 8157.95 160.73 o 7 10 0 4717.55 4644.97 107.74 o 8 10 0 5326.80 5243.19 111.34 o 9 10 0 52.43 59.60 13.89 o 10 10 0 34.95 95.72 38.01 o 11 10 0 70.25 200.01 151.58 o 12 10 0 680.44 581.60 75.34 o 13 10 0 6187.62 6136.76 330.13 o 14 10 0 267.26 240.65 127.88 o -9 11 0 902.84 848.62 90.59 o -8 11 0 37.03 72.42 80.41 o -7 11 0 2512.50 2488.81 129.23 o -6 11 0 17.59 82.20 80.87 o -5 11 0 8800.39 9034.16 255.08 o -4 11 0 3930.15 3795.56 119.54 o -3 11 0 2267.96 2447.32 88.82 o -2 11 0 22132.63 22324.67 485.28 o -1 11 0 37.64 51.05 44.71 o 0 11 0 49514.64 48991.90 939.23 o 1 11 0 2187.96 2097.54 59.69 o 2 11 0 9438.25 9235.91 189.53 o 3 11 0 8950.37 8998.45 150.27 o 4 11 0 196.19 257.95 25.62 o 5 11 0 72.64 117.25 23.16 o 6 11 0 677.69 675.80 36.51 o 7 11 0 1076.16 1093.58 38.06 o 8 11 0 2461.46 2292.02 84.89 o 9 11 0 7970.59 7539.27 206.32 o 10 11 0 7627.53 7332.49 352.57 o 11 11 0 309.06 409.46 68.10 o 12 11 0 6318.14 6401.58 360.59 o 13 11 0 437.12 371.30 100.21 o 14 11 0 10237.54 10333.86 504.84 o -8 12 0 4802.98 4590.44 215.14 o -7 12 0 3031.54 2860.09 143.44 o -6 12 0 5697.60 5606.28 220.03 o -5 12 0 11380.13 11377.73 407.76 o -4 12 0 4589.31 4787.54 186.00 o -3 12 0 19106.23 19464.28 477.26 o -2 12 0 2477.20 2500.43 103.10 o -1 12 0 15972.27 16582.27 400.37 o 0 12 0 4292.12 4108.03 196.03 o 1 12 0 3998.80 4138.44 129.68 o 2 12 0 3026.03 3008.78 93.46 o 3 12 0 45.18 33.16 33.78 o 4 12 0 533.28 543.05 33.71 o 5 12 0 63.52 103.77 20.47 o 6 12 0 7574.26 7196.55 184.39 o 7 12 0 3416.41 3252.37 148.19 o 8 12 0 3261.47 3430.09 105.15 o 9 12 0 16585.25 17074.98 458.27 o 10 12 0 91.10 54.11 146.62 o 11 12 0 14774.66 13753.26 789.73 o 12 12 0 1911.23 1910.88 154.54 o 13 12 0 8513.38 8424.30 458.05 o -7 13 0 1899.71 1992.16 132.03 o -6 13 0 16191.87 15922.29 716.56 o -5 13 0 148.08 171.55 64.54 o -4 13 0 11318.67 11670.53 374.66 o -3 13 0 1684.17 1835.47 132.99 o -2 13 0 3895.57 4039.05 168.07 o -1 13 0 3324.40 3401.12 153.36 o 0 13 0 667.53 677.71 61.60 o 1 13 0 200.44 252.04 62.92 o 2 13 0 196.76 231.80 56.41 o 3 13 0 520.47 577.66 53.41 o 4 13 0 89.34 120.29 32.18 o 5 13 0 18411.00 18790.83 443.88 o 6 13 0 7453.75 7109.72 211.55 o 7 13 0 7624.80 7823.09 244.31 o 8 13 0 15522.76 16021.13 441.27 o 9 13 0 631.90 684.95 84.48 o 10 13 0 11117.42 12411.24 529.61 o 11 13 0 4150.30 3522.59 242.13 o 12 13 0 2927.35 2995.89 203.17 o 13 13 0 1677.05 1355.34 144.85 o -6 14 0 817.96 639.51 100.25 o -5 14 0 5646.42 5365.19 241.26 o -4 14 0 296.69 316.19 66.94 o -3 14 0 73.79 4.42 72.40 o -2 14 0 92.30 165.76 84.11 o -1 14 0 54.41 142.68 70.20 o 0 14 0 3603.04 3576.96 194.37 o 1 14 0 739.21 685.14 96.77 o 2 14 0 5550.25 5396.22 239.09 o 3 14 0 4013.74 4025.37 189.49 o 4 14 0 8516.20 8110.14 441.77 o 5 14 0 11342.93 11069.81 475.68 o 6 14 0 372.07 338.76 56.21 o 7 14 0 9512.01 9278.62 350.95 o 8 14 0 133.45 156.21 76.31 o 9 14 0 11115.34 11445.88 480.88 o 10 14 0 1692.80 1499.27 101.92 o 11 14 0 464.90 441.24 80.58 o 12 14 0 353.65 217.07 100.22 o -5 15 0 7.75 29.32 74.79 o -4 15 0 74.87 121.99 69.07 o -3 15 0 1491.58 1367.87 121.75 o -2 15 0 106.32 30.12 82.90 o -1 15 0 9224.68 8887.40 347.65 o 0 15 0 2388.28 2194.06 214.34 o 1 15 0 11149.64 11186.21 521.10 o 2 15 0 10800.86 10531.49 636.09 o 3 15 0 2587.46 2705.01 190.55 o 4 15 0 14396.55 14191.63 720.88 o 5 15 0 228.23 305.14 88.62 o 6 15 0 5637.70 5514.26 227.79 o 7 15 0 3305.32 3151.36 181.12 o 8 15 0 332.69 438.28 96.82 o 9 15 0 424.86 358.10 83.69 o 10 15 0 33.85 43.91 56.83 o 11 15 0 587.21 454.21 72.27 o -3 16 0 129.22 300.70 136.98 o -2 16 0 7362.01 7135.46 339.94 o -1 16 0 3818.48 4001.17 246.98 o 0 16 0 9204.84 9137.81 439.52 o 1 16 0 9854.29 9571.48 643.35 o 2 16 0 54.92 -3.13 71.44 o 3 16 0 16202.15 15443.53 985.03 o 4 16 0 473.90 496.30 83.46 o 5 16 0 4577.63 4561.27 358.75 o 6 16 0 625.02 659.23 89.93 o 7 16 0 69.20 46.11 83.90 o 8 16 0 832.83 821.14 148.52 o 9 16 0 408.05 354.05 64.95 o 10 16 0 2065.35 1826.59 173.60 o -1 17 0 4191.57 3657.46 249.99 o 0 17 0 6319.00 6619.48 374.39 o 1 17 0 535.04 390.33 279.25 o 2 17 0 1645.97 1657.78 182.17 o 3 17 0 369.41 220.92 83.33 o 4 17 0 1333.94 1267.26 180.65 o 5 17 0 2.61 11.67 150.74 o 6 17 0 135.94 131.87 117.62 o 7 17 0 3114.57 2791.12 228.86 o 8 17 0 24.83 109.01 56.29 o 9 17 0 7423.87 7193.44 857.15 o 2 18 0 334.11 224.20 127.96 o 3 18 0 156.68 219.94 194.54 o 4 18 0 2319.89 2193.00 249.33 o 5 18 0 211.71 -107.43 280.54 o 6 18 0 6608.89 6024.56 438.02 o -4 -18 1 241.98 395.86 107.45 o -3 -18 1 755.03 706.52 88.65 o -8 -17 1 7222.75 7060.16 490.63 o -7 -17 1 1159.06 1102.54 110.70 o -6 -17 1 861.83 677.66 157.03 o -5 -17 1 43.97 9.92 47.69 o -4 -17 1 146.01 94.12 69.22 o -3 -17 1 143.27 145.67 104.60 o -2 -17 1 43.01 58.51 101.73 o -1 -17 1 5067.48 4047.94 291.01 o 0 -17 1 525.57 365.53 104.55 o 1 -17 1 5390.20 4850.02 377.00 o -10 -16 1 100.98 -194.30 394.28 o -9 -16 1 3748.97 4056.43 520.02 o -8 -16 1 828.48 842.13 122.08 o -7 -16 1 579.85 646.11 232.20 o -6 -16 1 29.46 22.34 52.34 o -5 -16 1 1523.93 1345.25 181.53 o -4 -16 1 5842.32 5447.67 542.57 o -3 -16 1 306.47 289.25 69.47 o -2 -16 1 8717.96 8481.31 739.15 o -1 -16 1 1809.57 2038.28 166.86 o 0 -16 1 7877.61 7741.49 393.61 o 1 -16 1 12113.22 12469.80 638.90 o 2 -16 1 1350.87 1653.64 152.19 o 3 -16 1 7741.33 7673.59 464.08 o -11 -15 1 14.32 -61.80 480.17 o -10 -15 1 36.56 82.93 94.80 o -9 -15 1 753.09 681.68 81.88 o -8 -15 1 104.97 78.41 47.89 o -7 -15 1 152.54 229.62 75.32 o -6 -15 1 688.32 666.97 104.24 o -5 -15 1 11666.12 11160.84 560.16 o -4 -15 1 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