# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2010src0043 _shelx_title ' 2010src0043 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 226.04 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.7701 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.0905 _cell_length_b 12.7583 _cell_length_c 14.4492 _cell_angle_alpha 100.026 _cell_angle_beta 98.124 _cell_angle_gamma 108.201 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4594.87 5568.07 286.48 o 3 0 0 28947.16 29448.64 1198.11 o 4 0 0 19263.62 19315.43 902.27 o 5 0 0 8540.55 8717.53 282.52 o 6 0 0 1399.38 1295.27 42.13 o 7 0 0 1408.75 1357.50 52.82 o 8 0 0 2700.54 2880.37 80.72 o 9 0 0 1212.55 1408.31 128.22 o 10 0 0 218.31 191.44 175.38 o 11 0 0 103.09 -9.44 63.72 o -12 1 0 421.07 480.55 90.51 o -11 1 0 910.82 1167.54 86.31 o -10 1 0 1531.42 1710.31 108.70 o -9 1 0 3083.84 2986.83 282.07 o -8 1 0 4704.56 4544.43 212.10 o -7 1 0 3700.25 2858.36 178.00 o -6 1 0 3391.64 3402.81 160.14 o -5 1 0 13950.74 9677.69 1026.10 o -4 1 0 22949.77 22244.78 1106.18 o -3 1 0 1067.80 501.20 97.43 o -2 1 0 7342.80 7795.86 547.66 o 1 1 0 18637.18 21574.80 755.39 o 2 1 0 20563.55 22013.63 506.10 o 3 1 0 23260.42 25717.78 703.91 o 4 1 0 9021.33 9026.38 222.36 o 5 1 0 11.18 168.83 28.54 o 6 1 0 67.86 97.70 38.19 o 7 1 0 235.08 224.13 34.85 o 8 1 0 1215.09 1173.14 67.09 o 9 1 0 741.49 663.74 52.35 o 11 1 0 94.01 11.27 59.60 o -12 2 0 927.36 1199.64 100.26 o -11 2 0 825.26 900.94 77.11 o -10 2 0 3094.75 3273.11 242.01 o -9 2 0 8222.35 8530.64 359.14 o -8 2 0 3369.72 3501.32 141.16 o -7 2 0 152.65 133.04 61.85 o -6 2 0 6003.08 5947.64 369.80 o -5 2 0 14451.73 13782.01 2266.78 o -4 2 0 4810.38 4702.26 348.59 o -3 2 0 282.12 205.17 29.43 o -2 2 0 4011.81 3694.91 116.30 o -1 2 0 875.36 711.41 26.71 o 0 2 0 154.66 231.02 19.09 o 1 2 0 5056.89 7196.61 238.86 o 2 2 0 598.89 878.34 38.81 o 3 2 0 1771.96 2142.10 63.00 o 4 2 0 5340.30 6251.82 167.01 o 5 2 0 2721.72 3203.16 118.81 o 6 2 0 2261.07 2340.21 75.03 o 7 2 0 2684.00 2864.02 131.18 o 8 2 0 7508.23 7361.30 232.19 o 9 2 0 4712.79 4558.80 217.11 o 10 2 0 1442.83 1226.81 102.70 o 11 2 0 1323.34 1343.88 490.21 o -12 3 0 764.64 1208.12 98.24 o -11 3 0 2164.32 2525.95 143.59 o -10 3 0 6065.17 6501.62 318.21 o -9 3 0 4221.86 3917.05 332.67 o -8 3 0 919.56 841.49 231.36 o -7 3 0 1635.33 1428.25 102.81 o -6 3 0 3975.71 4106.19 277.68 o -5 3 0 1364.60 1321.53 136.19 o -4 3 0 117.91 109.22 44.31 o -3 3 0 2628.46 2752.37 140.84 o -2 3 0 793.29 882.23 29.45 o -1 3 0 1110.88 847.14 32.46 o 0 3 0 91.65 204.44 25.36 o 1 3 0 4997.20 6129.19 185.23 o 2 3 0 3184.23 4151.78 140.39 o 3 3 0 9167.77 11616.55 345.70 o 4 3 0 15330.96 16581.52 483.54 o 5 3 0 8285.67 8364.07 230.78 o 6 3 0 5026.12 5195.41 162.56 o 7 3 0 5751.96 5833.51 214.56 o 8 3 0 7976.31 7916.51 292.93 o 9 3 0 5343.17 5227.75 336.98 o 10 3 0 879.27 833.05 270.83 o 11 3 0 907.31 1330.63 532.00 o -12 4 0 744.27 753.56 87.56 o -11 4 0 2298.82 2527.26 136.39 o -10 4 0 4027.52 4746.15 276.78 o -9 4 0 1232.68 991.50 116.51 o -8 4 0 25.14 -80.23 193.08 o -7 4 0 162.36 206.49 93.07 o -6 4 0 88.11 571.35 179.85 o -5 4 0 5622.46 5237.20 165.56 o -4 4 0 1450.47 1413.42 65.41 o -3 4 0 118.70 109.29 28.58 o -2 4 0 11340.92 10999.37 278.56 o -1 4 0 10294.05 10613.52 317.88 o 0 4 0 5873.16 7020.97 196.30 o 1 4 0 4538.03 5470.85 157.79 o 2 4 0 1600.87 1960.39 104.47 o 3 4 0 7487.24 8486.13 274.15 o 4 4 0 10083.64 11948.43 407.26 o 5 4 0 3520.36 3736.14 105.43 o 6 4 0 1854.70 1903.34 66.84 o 7 4 0 4096.78 3683.49 239.91 o 8 4 0 4157.32 4304.72 235.51 o 9 4 0 1569.26 1149.12 199.22 o 10 4 0 171.37 147.00 71.38 o -12 5 0 61.15 213.17 105.39 o -11 5 0 156.52 273.29 147.43 o -10 5 0 6.16 133.12 77.65 o -9 5 0 173.04 295.13 88.02 o -8 5 0 1423.01 1814.25 156.93 o -7 5 0 2735.80 2844.02 180.77 o -6 5 0 4258.15 3752.41 116.75 o -5 5 0 14282.58 13555.52 468.68 o -4 5 0 8124.35 7849.57 250.65 o -3 5 0 18134.18 16439.88 405.01 o -2 5 0 22621.76 21041.90 520.93 o -1 5 0 23777.36 26379.36 817.14 o 0 5 0 8828.93 10237.13 266.93 o 1 5 0 1925.73 2197.92 72.96 o 2 5 0 8561.42 9431.03 276.80 o 3 5 0 7181.50 7982.93 257.38 o 4 5 0 5865.79 6557.62 202.67 o 5 5 0 1286.52 1411.28 60.56 o 6 5 0 938.16 895.56 63.83 o 7 5 0 1283.99 1318.97 94.67 o 8 5 0 328.61 286.60 97.32 o 9 5 0 109.65 373.63 83.58 o 10 5 0 13.69 5.61 159.95 o -12 6 0 585.89 675.27 102.83 o -11 6 0 564.30 809.17 160.68 o -10 6 0 2175.96 2521.44 205.63 o -9 6 0 2054.24 2102.41 160.47 o -8 6 0 2685.65 2955.94 442.93 o -7 6 0 8426.91 8397.05 230.20 o -6 6 0 10943.13 10042.12 331.05 o -5 6 0 18620.87 17893.47 438.13 o -4 6 0 18344.23 18614.46 796.76 o -3 6 0 9586.26 8887.00 219.36 o -2 6 0 28100.50 29552.40 1185.46 o -1 6 0 14808.38 15878.52 459.23 o 0 6 0 6047.52 6828.35 196.96 o 1 6 0 5129.36 5807.68 180.23 o 2 6 0 3532.78 3632.90 158.42 o 3 6 0 1764.43 1725.68 79.28 o 4 6 0 339.04 244.41 41.74 o 5 6 0 371.10 338.10 42.77 o 6 6 0 0.81 56.24 49.42 o 7 6 0 35.23 148.21 98.61 o 8 6 0 30.82 -83.66 79.66 o 9 6 0 37.65 214.37 80.58 o -12 7 0 1178.45 1401.75 101.63 o -11 7 0 2181.09 2639.37 249.38 o -10 7 0 1663.14 1518.28 141.73 o -9 7 0 696.55 590.80 68.22 o -8 7 0 1266.93 1317.29 51.22 o -7 7 0 5244.01 5011.89 138.22 o -6 7 0 10012.61 10092.91 238.91 o -5 7 0 3423.17 3529.44 106.76 o -4 7 0 1490.46 1458.83 55.69 o -3 7 0 5748.46 5650.09 149.18 o -2 7 0 15048.05 14735.52 404.28 o -1 7 0 488.08 430.09 29.58 o 0 7 0 17.32 -12.17 44.09 o 1 7 0 6.19 61.72 46.40 o 2 7 0 216.48 282.88 42.29 o 3 7 0 972.30 1164.30 77.87 o 4 7 0 679.27 707.60 66.29 o 5 7 0 883.01 814.47 57.13 o 6 7 0 1604.24 1397.14 86.57 o 7 7 0 1272.20 1024.91 134.13 o 8 7 0 916.52 964.22 119.35 o 9 7 0 396.52 466.25 108.38 o -12 8 0 1820.76 1965.33 179.80 o -11 8 0 2147.95 2566.08 163.75 o -10 8 0 2455.39 2825.43 163.98 o -9 8 0 303.78 289.23 81.61 o -8 8 0 521.17 572.47 55.99 o -7 8 0 1437.94 1456.89 48.37 o -6 8 0 252.02 235.27 59.33 o -5 8 0 140.30 106.15 57.02 o -4 8 0 52.64 12.54 27.96 o -3 8 0 17.54 67.16 26.14 o -2 8 0 344.89 313.10 41.35 o -1 8 0 264.71 252.10 30.21 o 0 8 0 1333.75 1405.68 66.29 o 1 8 0 5186.43 5576.24 187.19 o 2 8 0 4367.84 4685.44 217.19 o 3 8 0 4930.11 5338.20 195.31 o 4 8 0 3679.57 4191.91 171.44 o 5 8 0 2818.89 2387.53 142.42 o 6 8 0 4723.43 4831.04 257.20 o 7 8 0 2408.12 2386.52 136.12 o 8 8 0 1270.47 1193.91 179.99 o -12 9 0 1962.37 2682.53 259.93 o -11 9 0 1967.97 2734.50 219.60 o -10 9 0 664.53 653.96 63.39 o -9 9 0 64.37 132.44 18.17 o -8 9 0 170.64 247.06 82.23 o -7 9 0 72.09 1884.85 1060.47 o -6 9 0 169.65 212.96 43.58 o -5 9 0 82.57 142.06 32.11 o -4 9 0 312.77 384.82 39.23 o -3 9 0 3918.28 3722.32 121.37 o -2 9 0 1417.48 1444.21 69.24 o -1 9 0 1127.04 954.13 51.43 o 0 9 0 2079.05 2128.31 94.70 o 1 9 0 4636.82 5183.36 198.16 o 2 9 0 4762.72 4876.39 250.91 o 3 9 0 3389.51 3446.70 161.05 o 4 9 0 3823.12 4660.95 237.95 o 5 9 0 2126.99 1695.81 119.00 o 6 9 0 2667.62 2693.14 199.66 o 7 9 0 1293.01 1465.32 313.65 o -12 10 0 289.09 1511.73 465.20 o -11 10 0 16.73 692.04 411.01 o -10 10 0 16.14 -7.98 90.77 o -9 10 0 268.14 369.70 191.05 o -8 10 0 638.05 819.03 54.57 o -7 10 0 1472.54 1350.68 143.60 o -6 10 0 1054.45 1091.28 57.94 o -5 10 0 786.32 807.49 65.95 o -4 10 0 2250.37 2094.47 78.24 o -3 10 0 3862.84 3852.35 146.05 o -2 10 0 545.47 500.56 53.61 o -1 10 0 2072.09 1669.08 121.36 o 0 10 0 1391.51 1392.12 125.50 o 1 10 0 3703.45 3662.64 170.37 o 2 10 0 3739.39 3955.01 236.77 o 3 10 0 1467.28 1551.19 97.10 o 4 10 0 464.00 404.82 64.86 o 5 10 0 387.19 355.11 81.41 o 6 10 0 1121.51 958.41 132.97 o -12 11 0 442.34 945.59 542.82 o -11 11 0 636.67 229.01 404.83 o -10 11 0 1133.04 1163.72 202.76 o -9 11 0 2472.74 2376.32 285.34 o -8 11 0 5719.02 5901.35 260.09 o -7 11 0 7610.16 7413.44 255.90 o -6 11 0 3053.98 3058.80 225.64 o -5 11 0 5920.23 5923.30 218.29 o -4 11 0 8111.86 7967.41 271.52 o -3 11 0 4858.37 4703.47 184.28 o -2 11 0 2184.04 2292.42 127.39 o -1 11 0 1997.87 1890.57 385.99 o 0 11 0 1287.97 1077.43 159.41 o 1 11 0 806.60 602.86 71.25 o 2 11 0 1328.87 1557.36 150.16 o 3 11 0 625.90 435.35 57.17 o 4 11 0 64.74 24.18 98.65 o 5 11 0 80.05 -177.77 118.52 o -11 12 0 1284.72 1399.81 164.99 o -10 12 0 1538.87 1461.94 148.45 o -9 12 0 5381.57 6263.85 353.92 o -8 12 0 4588.37 4727.76 319.37 o -7 12 0 6279.25 6032.90 227.83 o -6 12 0 3479.30 3252.20 144.59 o -5 12 0 2298.71 2442.51 134.12 o -4 12 0 4766.16 4593.28 194.84 o -3 12 0 5860.44 5283.31 232.91 o -2 12 0 1836.81 1635.17 93.94 o -1 12 0 483.17 371.48 111.39 o 0 12 0 136.01 336.97 145.32 o 1 12 0 312.66 349.59 85.04 o 2 12 0 98.21 -104.59 80.71 o 3 12 0 4.77 193.13 104.32 o 4 12 0 19.65 145.32 160.47 o -10 13 0 601.02 905.82 155.00 o -9 13 0 1416.79 1438.11 169.20 o -8 13 0 1541.46 1598.10 103.13 o -7 13 0 1122.29 1211.36 119.46 o -6 13 0 1456.81 1442.64 81.98 o -5 13 0 270.75 208.58 53.79 o -4 13 0 7.64 92.92 68.32 o -3 13 0 97.87 238.56 73.57 o -2 13 0 487.86 708.33 99.12 o -1 13 0 258.99 29.08 76.47 o 0 13 0 165.95 140.06 88.05 o 1 13 0 851.15 988.73 115.21 o 2 13 0 434.20 379.25 258.35 o 3 13 0 202.91 162.86 140.07 o -10 14 0 8.82 137.67 112.39 o -9 14 0 42.17 -82.14 202.44 o -8 14 0 38.23 766.23 496.75 o -7 14 0 1.83 115.41 107.34 o -6 14 0 287.33 204.41 57.54 o -5 14 0 12.89 172.15 70.73 o -4 14 0 319.33 239.17 61.42 o -3 14 0 2028.33 2269.98 187.89 o -2 14 0 1023.97 627.72 152.92 o -1 14 0 2288.36 2180.18 178.83 o 0 14 0 2983.45 2513.89 214.93 o 1 14 0 3228.62 2362.25 224.97 o 2 14 0 1965.26 1440.90 246.63 o -8 15 0 300.02 47.07 78.37 o -7 15 0 422.63 193.76 117.67 o -6 15 0 906.62 805.96 135.06 o -5 15 0 941.09 879.89 88.90 o -4 15 0 669.71 686.14 84.61 o -3 15 0 666.05 462.82 118.04 o -2 15 0 1029.83 409.79 129.23 o -1 15 0 1453.70 1509.49 135.16 o 0 15 0 2475.10 2327.50 282.97 o -6 16 0 611.02 1001.39 158.15 o -5 16 0 1432.87 1433.99 117.81 o -4 16 0 1492.80 1393.46 132.00 o -3 16 0 834.05 322.30 147.59 o 2 -16 1 134.20 548.82 108.65 o 3 -16 1 4.84 113.83 93.11 o 4 -16 1 194.87 203.85 129.78 o 5 -16 1 1.37 201.05 82.16 o 6 -16 1 3.36 -128.68 85.79 o 7 -16 1 35.79 103.21 161.47 o 0 -15 1 57.45 212.78 93.45 o 1 -15 1 12.78 115.56 88.71 o 2 -15 1 231.72 266.34 103.90 o 3 -15 1 497.05 410.53 221.86 o 4 -15 1 1056.09 697.97 97.12 o 5 -15 1 689.71 662.71 80.32 o 6 -15 1 144.35 125.26 126.89 o 7 -15 1 574.21 604.77 151.93 o 8 -15 1 1217.01 1336.74 163.63 o -2 -14 1 144.35 143.65 57.61 o -1 -14 1 696.78 696.25 73.04 o 0 -14 1 963.00 983.97 97.18 o 1 -14 1 841.88 724.14 116.80 o 2 -14 1 1215.56 1020.10 175.98 o 3 -14 1 3524.85 3441.44 269.32 o 4 -14 1 3095.46 3382.06 184.47 o 5 -14 1 3102.92 3572.04 236.31 o 6 -14 1 2439.74 2579.29 235.99 o 7 -14 1 1909.33 1929.51 110.21 o 8 -14 1 2223.47 2547.11 362.85 o 9 -14 1 472.52 458.77 117.23 o 10 -14 1 492.66 441.29 99.52 o -4 -13 1 146.57 214.60 153.76 o -3 -13 1 826.95 677.11 126.54 o -2 -13 1 1591.57 1340.74 147.18 o -1 -13 1 1873.01 1421.91 116.13 o 0 -13 1 1435.05 1448.15 106.37 o 1 -13 1 1269.10 1330.67 92.50 o 2 -13 1 4344.72 4805.71 332.17 o 3 -13 1 6269.55 6371.15 347.78 o 4 -13 1 4446.82 4278.87 235.14 o 5 -13 1 1969.22 1718.07 163.13 o 6 -13 1 3828.68 3757.08 208.10 o 7 -13 1 2281.65 2132.50 117.48 o 8 -13 1 489.06 391.83 83.45 o 9 -13 1 1051.40 1334.74 107.18 o 10 -13 1 672.92 404.66 428.10 o -4 -12 1 187.87 163.13 100.38 o -3 -12 1 1102.24 879.76 114.28 o -2 -12 1 3299.62 3123.00 229.55 o -1 -12 1 2567.66 2543.25 206.16 o 0 -12 1 762.71 751.24 62.05 o 1 -12 1 1493.91 1802.53 109.15 o 2 -12 1 2402.61 2286.24 335.37 o 3 -12 1 1201.48 1048.46 109.56 o 4 -12 1 653.78 779.35 87.51 o 5 -12 1 960.75 1245.72 84.95 o 6 -12 1 595.28 848.15 65.66 o 7 -12 1 3.91 70.37 66.12 o 8 -12 1 34.15 325.62 209.75 o 9 -12 1 19.58 197.56 254.55 o 11 -12 1 1023.32 134.87 443.51 o -6 -11 1 1655.17 1559.59 149.14 o -5 -11 1 1555.01 1282.63 152.47 o -4 -11 1 83.59 -25.75 137.78 o -3 -11 1 804.95 717.16 69.98 o -2 -11 1 2097.29 1908.30 155.30 o -1 -11 1 514.98 319.58 53.76 o 0 -11 1 579.90 569.00 92.16 o 1 -11 1 1274.20 1204.95 74.88 o 2 -11 1 287.55 282.43 40.72 o 3 -11 1 111.26 174.56 64.37 o 4 -11 1 55.75 226.94 54.42 o 5 -11 1 133.75 222.95 49.73 o 6 -11 1 1309.04 1162.82 65.45 o 7 -11 1 2563.65 2658.03 144.70 o 8 -11 1 2016.50 1900.77 152.77 o 9 -11 1 972.23 1104.06 100.82 o 10 -11 1 1818.96 1764.96 130.05 o 11 -11 1 3782.28 4408.53 645.66 o -7 -10 1 2108.65 1899.20 209.12 o -6 -10 1 1288.07 1233.86 213.25 o -5 -10 1 1493.70 1420.10 121.97 o -4 -10 1 1583.94 1544.72 114.03 o -3 -10 1 642.95 550.55 78.60 o -2 -10 1 6.22 13.85 61.31 o -1 -10 1 133.44 116.75 49.64 o 0 -10 1 19.97 -20.63 40.63 o 1 -10 1 24.30 94.95 27.99 o 2 -10 1 868.45 786.57 39.03 o 3 -10 1 900.48 974.99 57.64 o 4 -10 1 382.84 265.67 46.16 o 5 -10 1 65.57 123.55 74.38 o 6 -10 1 4058.68 4296.94 151.24 o 7 -10 1 3775.94 3989.05 136.96 o 8 -10 1 1380.36 1493.01 75.15 o 9 -10 1 1325.38 1292.32 79.87 o 10 -10 1 2287.71 2489.83 150.42 o 11 -10 1 4027.73 4353.46 335.71 o 12 -10 1 2122.30 2272.32 217.14 o -7 -9 1 412.72 109.69 223.89 o -6 -9 1 188.64 40.84 117.14 o -5 -9 1 288.95 266.28 45.72 o -4 -9 1 185.09 256.20 41.61 o -3 -9 1 35.31 2.59 49.73 o -2 -9 1 1837.68 1757.32 88.32 o -1 -9 1 293.24 262.33 46.79 o 0 -9 1 886.10 839.77 52.76 o 1 -9 1 5987.38 6409.68 212.03 o 2 -9 1 9266.25 8981.96 218.16 o 3 -9 1 5008.11 5036.22 135.69 o 4 -9 1 1507.67 1260.37 63.15 o 5 -9 1 2123.89 2018.96 63.18 o 6 -9 1 3032.27 2924.90 109.70 o 7 -9 1 1740.89 1744.38 71.52 o 8 -9 1 1483.85 1450.38 53.48 o 9 -9 1 1303.03 1278.46 47.98 o 10 -9 1 1505.78 1578.32 106.38 o 11 -9 1 1063.46 1063.34 197.49 o 12 -9 1 358.96 585.19 126.17 o -8 -8 1 1.56 -50.90 106.42 o -7 -8 1 919.27 739.64 136.73 o -6 -8 1 836.70 722.82 69.58 o -5 -8 1 66.43 204.79 38.97 o -4 -8 1 2094.58 1975.97 119.57 o -3 -8 1 8303.45 8908.01 336.47 o -2 -8 1 6933.27 7124.45 229.45 o -1 -8 1 5194.15 5240.75 293.19 o 0 -8 1 3815.41 3975.08 129.78 o 1 -8 1 19523.91 19974.92 588.62 o 2 -8 1 21299.46 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